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Search for "scanning electron microscopy" in Full Text gives 665 result(s) in Beilstein Journal of Nanotechnology. Showing first 200.

Photocatalytic degradation of methylene blue under visible light by cobalt ferrite nanoparticles/graphene quantum dots

  • Vo Chau Ngoc Anh,
  • Le Thi Thanh Nhi,
  • Le Thi Kim Dung,
  • Dang Thi Ngoc Hoa,
  • Nguyen Truong Son,
  • Nguyen Thi Thao Uyen,
  • Nguyen Ngoc Uyen Thu,
  • Le Van Thanh Son,
  • Le Trung Hieu,
  • Tran Ngoc Tuyen and
  • Dinh Quang Khieu

Beilstein J. Nanotechnol. 2024, 15, 475–489, doi:10.3762/bjnano.15.43

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  • Tristar-3030 system (Micromeritics, USA). The magnetic properties were measured on a Micro Sense vibrating-sample magnetometer (VSM) at room temperature. Scanning electron microscopy (SEM) observations and energy-dispersive X-ray elemental mapping (EDX mapping) were carried out on a Hitachi S-4800 FESEM
  • electron microscopy, transmission electron microscopy, ultraviolet–visible diffuse reflectance spectroscopy, Fourier-transform infrared spectroscopy, photoluminescence spectroscopy, vibrating-sample magnetometry, and nitrogen adsorption/desorption isotherms. Cobalt ferrite crystals of around 8–10 nm and
  • synthesize cobalt ferrite nanoparticles/graphene quantum dots (CF/GQDs). The material was prepared from a homogeneous mixture of iron nitrate, cobalt nitrate, and starch at 140, 180 and 200 °C in a 24 h thermal hydrolysis process. The obtained materials were characterised by using X-ray diffraction, scanning
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Published 29 Apr 2024

Fabrication of nanocrystal forms of ᴅ-cycloserine and their application for transdermal and enteric drug delivery systems

  • Hsuan-Ang Tsai,
  • Tsai-Miao Shih,
  • Theodore Tsai,
  • Jhe-Wei Hu,
  • Yi-An Lai,
  • Jui-Fu Hsiao and
  • Guochuan Emil Tsai

Beilstein J. Nanotechnol. 2024, 15, 465–474, doi:10.3762/bjnano.15.42

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  • formulation in the transdermal delivery system. Scanning electron microscopy images of commercial DCS (A) and DCS nanocrystals (B). The X-ray powder diffraction spectra of DCD nanocrystal and commercial DCS. The pH stability test of DCS in neutral (pH 7.4) and acidic (pH 1.2) environments (p < 0.01). In vitro
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Published 25 Apr 2024

Heat-induced morphological changes in silver nanowires deposited on a patterned silicon substrate

  • Elyad Damerchi,
  • Sven Oras,
  • Edgars Butanovs,
  • Allar Liivlaid,
  • Mikk Antsov,
  • Boris Polyakov,
  • Annamarija Trausa,
  • Veronika Zadin,
  • Andreas Kyritsakis,
  • Loïc Vidal,
  • Karine Mougin,
  • Siim Pikker and
  • Sergei Vlassov

Beilstein J. Nanotechnol. 2024, 15, 435–446, doi:10.3762/bjnano.15.39

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  • process, fragmentation in either adhered or suspended parts can dominate. Experiments were supported by finite element method and molecular dynamics simulations. Keywords: diffusion; finite element method; heat treatment; molecular dynamics simulations; morphological changes; scanning electron microscopy
  • the results from the scheme 1. Approximately one hour waiting time between cycles was chosen to give enough time for taking series of scanning electron microscopy (SEM, FEI, Nanosem 450) images after each heating cycle. Additionally, a separate series of transmission electron microscopy (TEM
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Published 22 Apr 2024

Insect attachment on waxy plant surfaces: the effect of pad contamination by different waxes

  • Elena V. Gorb and
  • Stanislav N. Gorb

Beilstein J. Nanotechnol. 2024, 15, 385–395, doi:10.3762/bjnano.15.35

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  • ) were tested. Scanning electron microscopy To visualize the waxy plant surfaces and attachment devices in the C. fastuosa male beetle in both clean and contaminated conditions, scanning electron microscopy was employed. For plant surfaces, small (ca. 1 cm2) pieces of plant organs were used. In the case
  • , experiments with all waxy plant surfaces (d.f. = 44) and (2) data obtained from five test insects on each plant surface separately (d.f. = 4). Scanning electron microscopy (SEM) micrographs of waxy plant surfaces in the young stem of Acer negundo (a) and adaxial (upper) leaf sides of Aloe vera (b), Aquilegia
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Published 11 Apr 2024

Modulated critical currents of spin-transfer torque-induced resistance changes in NiCu/Cu multilayered nanowires

  • Mengqi Fu,
  • Roman Hartmann,
  • Julian Braun,
  • Sergej Andreev,
  • Torsten Pietsch and
  • Elke Scheer

Beilstein J. Nanotechnol. 2024, 15, 360–366, doi:10.3762/bjnano.15.32

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  • device fabrication, and scanning electron microscopy (SEM) images of the devices during the fabrication process are presented in Supporting Information File 1. In most reported works, the nanowires were deposited in all pores of the AAO templates [18][19][20][21]. Additional etching steps or coating
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Published 03 Apr 2024

Comparative electron microscopy particle sizing of TiO2 pigments: sample preparation and measurement

  • Ralf Theissmann,
  • Christopher Drury,
  • Markus Rohe,
  • Thomas Koch,
  • Jochen Winkler and
  • Petr Pikal

Beilstein J. Nanotechnol. 2024, 15, 317–332, doi:10.3762/bjnano.15.29

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  • manufactured as a standard white pigment grade, which would be significantly inferior if more than 50% of its particles were below 100 nm in diameter. In other papers, samples of the same materials were measured using scanning electron microscopy (SEM) and found not to meet the EU classification for
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Published 25 Mar 2024

Ultrasensitive and ultrastretchable metal crack strain sensor based on helical polydimethylsiloxane

  • Shangbi Chen,
  • Dewen Liu,
  • Weiwei Chen,
  • Huajiang Chen,
  • Jiawei Li and
  • Jinfang Wang

Beilstein J. Nanotechnol. 2024, 15, 270–278, doi:10.3762/bjnano.15.25

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  • with PDMS. Parts of the experimental procedure are shown in Figure S6 (Supporting Information File 1). Characterization The surface morphology of the samples prepared in this study was examined through the utilization of scanning electron microscopy (SEM) (TESCAN MIRA3, Czech Republic) and an optical
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Published 01 Mar 2024

Graphene removal by water-assisted focused electron-beam-induced etching – unveiling the dose and dwell time impact on the etch profile and topographical changes in SiO2 substrates

  • Aleksandra Szkudlarek,
  • Jan M. Michalik,
  • Inés Serrano-Esparza,
  • Zdeněk Nováček,
  • Veronika Novotná,
  • Piotr Ozga,
  • Czesław Kapusta and
  • José María De Teresa

Beilstein J. Nanotechnol. 2024, 15, 190–198, doi:10.3762/bjnano.15.18

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  • studies: A) optical microscopy, B) scanning electron microscopy (SEM), C) AFM, and D) correlative probe and electron microscopy (CPEM). The optical contrast of graphene placed onto SiO2/Si allows us to easily distinguish between its mono-, bi-, triple, and thicker flakes layers. The values (approx. 2.5 nm
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Published 07 Feb 2024

Nanocarrier systems loaded with IR780, iron oxide nanoparticles and chlorambucil for cancer theragnostics

  • Phuong-Thao Dang-Luong,
  • Hong-Phuc Nguyen,
  • Loc Le-Tuan,
  • Xuan-Thang Cao,
  • Vy Tran-Anh and
  • Hieu Vu Quang

Beilstein J. Nanotechnol. 2024, 15, 180–189, doi:10.3762/bjnano.15.17

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  • were performed in both 0.1× PBS (13.7 mM of NaCl, 0.27 mM of KCl, 1 mM of Na2HPO4, and 0.18 mM of KH2PO4, pH 7.4) and animal cell culture media containing DMEM and 10% FBS. Scanning electron microscopy For scanning electron microscopy (SEM) experiments, 10 μL of F127-folate@NP was loaded on the silica
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Published 06 Feb 2024

Modification of graphene oxide and its effect on properties of natural rubber/graphene oxide nanocomposites

  • Nghiem Thi Thuong,
  • Le Dinh Quang,
  • Vu Quoc Cuong,
  • Cao Hong Ha,
  • Nguyen Ba Lam and
  • Seiichi Kawahara

Beilstein J. Nanotechnol. 2024, 15, 168–179, doi:10.3762/bjnano.15.16

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  • characterized by X-ray diffraction (XRD), Fourier-transform infrared spectroscopy, contact angle, thermal gravimetric analysis, and scanning electron microscopy. The XRD results showed the appearance of an amorphous region of silica particles at a diffraction angle of 22°. The formation of silica was
  • gravimetric analysis (TGA) of the samples was performed on a TA Q500 instrument. The temperature was increased at a heating rate of 10 °C /min from room temperature to 900 °C in air atmosphere. The morphology of the DPNR/GO-VTES was observed with field-emission scanning electron microscopy (FE-SEM) performed
  • efficiently attached to GO, and the attachment was more efficient in basic conditions rather than acidic conditions. Scanning electron microscopy images Figure 8 shows SEM images for GO-VTES(a) and GO-VTES(b). As can be seen, silica was produced with a size of approx. 50 nm for GO-VTES(a) and GO-VTES(b). It
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Published 05 Feb 2024

In situ optical sub-wavelength thickness control of porous anodic aluminum oxide

  • Aleksandrs Dutovs,
  • Raimonds Popļausks,
  • Oskars Putāns,
  • Vladislavs Perkanuks,
  • Aušrinė Jurkevičiūtė,
  • Tomas Tamulevičius,
  • Uldis Malinovskis,
  • Iryna Olyshevets,
  • Donats Erts and
  • Juris Prikulis

Beilstein J. Nanotechnol. 2024, 15, 126–133, doi:10.3762/bjnano.15.12

Graphical Abstract
  • materials in phase 2. A simulated annealing fitting algorithm was employed. The PAAO structure (Figure 1a) was confirmed using field-emission scanning electron microscopy (FE-SEM-4800, Hitachi, Tokyo, Japan). The relationship between thickness measurements using SEM and optical interferometry has been
  • Innovation Program under TRANSLATE project (Grant agreement: 964251). A. J. acknowledges support from European Regional Development Fund for postdoctoral project ”Patterned hybrid multilayer films for optical sensors” (no. 1.1.1.2/VIAA/4/20/615). (a) Scanning electron microscopy (SEM) micrograph showing top
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Published 31 Jan 2024

Assessing phytotoxicity and tolerance levels of ZnO nanoparticles on Raphanus sativus: implications for widespread adoptions

  • Pathirannahalage Sahan Samuditha,
  • Nadeesh Madusanka Adassooriya and
  • Nazeera Salim

Beilstein J. Nanotechnol. 2024, 15, 115–125, doi:10.3762/bjnano.15.11

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  • light scattering (DLS), and scanning electron microscopy (SEM). The effect of ZnO NPs (70 nm) on R. sativus grown in coir was evaluated. The application of 1,000 mg/L of ZnO NPs resulted in a significant increase (p < 0.05) in soluble protein content, carbohydrates, chlorophyll a (Chl-a), chlorophyll b
  • synthesized ZnO NPs were characterized via several techniques such as powder X-ray diffraction (PXRD), Fourier-transform infrared (FTIR) spectroscopy, solid-UV–vis spectroscopy, dynamic light scattering (DLS), and scanning electron microscopy (SEM). Then the potential phytotoxicity of the synthesized ZnO NPs
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Published 23 Jan 2024

New application of bimetallic Ag/Pt nanoplates in a colorimetric biosensor for specific detection of E. coli in water

  • Azam Bagheri Pebdeni,
  • Mohammad N. AL-Baiati and
  • Morteza Hosseini

Beilstein J. Nanotechnol. 2024, 15, 95–103, doi:10.3762/bjnano.15.9

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  • E. coli was successfully detected using the developed colorimetric sensor. The sensor offers a straightforward, sensitive, and dependable method for detecting pathogens and ensuring water safety. Results and Discussion Characterization of Ag/Pt NPL and apt-NPL Field-emission scanning electron
  • microscopy (FE-SEM) was used to investigate the form and shapes of NPLs. The size of the NPLs is approx. 42 nm. Figure 1a shows a combination of truncated triangular and circular plates of Ag/Pt NPLs. The NPLs were evenly distributed and shaped in the form of discs or triangles. Energy-dispersive X-ray
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Published 17 Jan 2024

Study of the reusability and stability of nylon nanofibres as an antibody immobilisation surface

  • Inés Peraile,
  • Matilde Gil-García,
  • Laura González-López,
  • Nushin A. Dabbagh-Escalante,
  • Juan C. Cabria-Ramos and
  • Paloma Lorenzo-Lozano

Beilstein J. Nanotechnol. 2024, 15, 83–94, doi:10.3762/bjnano.15.8

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  • immunocapture system in NF and 96-well microplate, for each time: ***p < 0.001. Field-emission scanning electron microscopy image of NFs. Acknowledgements We would like to thank the whole team at Nieves Murillo of TECNALIA – Industry and Transport Division for providing the nylon NFs. Funding These results
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Published 15 Jan 2024

Berberine-loaded polylactic acid nanofiber scaffold as a drug delivery system: The relationship between chemical characteristics, drug-release behavior, and antibacterial efficiency

  • Le Thi Le,
  • Hue Thi Nguyen,
  • Liem Thanh Nguyen,
  • Huy Quang Tran and
  • Thuy Thi Thu Nguyen

Beilstein J. Nanotechnol. 2024, 15, 71–82, doi:10.3762/bjnano.15.7

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  • observed by scanning electron microscopy (SEM, Figure 1). The BBR powder appeared as aggregates of rods in the micrometer size (Figure 1a), while BBR NPs were formed as nanoscale rectangles (Figure 1b). The electrospun PLA nanofibers showed bead-free and uniform morphology with fiber diameter in the range
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Published 12 Jan 2024

Influence of conductive carbon and MnCo2O4 on morphological and electrical properties of hydrogels for electrochemical energy conversion

  • Sylwia Pawłowska,
  • Karolina Cysewska,
  • Yasamin Ziai,
  • Jakub Karczewski,
  • Piotr Jasiński and
  • Sebastian Molin

Beilstein J. Nanotechnol. 2024, 15, 57–70, doi:10.3762/bjnano.15.6

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  • structures were examined in terms of their morphology, electrical properties, and catalytic layers in the OER process. Results and Discussion Characterisation of hydrogel-based polymer composites with dispersed catalytic and conductive particles Scanning electron microscopy (SEM) analysis of hydrogel samples
  • omitted, which is an element that distinguishes the applied procedure from others described in most literature reports. Scanning electron microscopy studies confirmed the fabrication of a composite polymer containing MCO catalyst particles and conductive carbon cCB particles either caught inside or bound
  • temperature above LCST results in shrinkage of the hydrogel structure and formation of inhomogeneities. Such a hydrogel ceases to be transparent and loses most of its water [42]. Morphological and physicochemical characterisation Scanning electron microscopy was performed with an FE-SEM FEI Quanta FEG 250 at
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Published 11 Jan 2024

Curcumin-loaded nanostructured systems for treatment of leishmaniasis: a review

  • Douglas Dourado,
  • Thayse Silva Medeiros,
  • Éverton do Nascimento Alencar,
  • Edijane Matos Sales and
  • Fábio Rocha Formiga

Beilstein J. Nanotechnol. 2024, 15, 37–50, doi:10.3762/bjnano.15.4

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  • when treated by both nanoandi and nanocopa. Moreover, there was a decrease in lesion size and parasite load from the liver and spleen of mice treated with NE. In ultrastructural analysis performed by scanning electron microscopy, it was possible to observe morphological changes, oval aspect, and
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Published 04 Jan 2024

Measurements of dichroic bow-tie antenna arrays with integrated cold-electron bolometers using YBCO oscillators

  • Leonid S. Revin,
  • Dmitry A. Pimanov,
  • Alexander V. Chiginev,
  • Anton V. Blagodatkin,
  • Viktor O. Zbrozhek,
  • Andrey V. Samartsev,
  • Anastasia N. Orlova,
  • Dmitry V. Masterov,
  • Alexey E. Parafin,
  • Victoria Yu. Safonova,
  • Anna V. Gordeeva,
  • Andrey L. Pankratov,
  • Leonid S. Kuzmin,
  • Anatolie S. Sidorenko,
  • Silvia Masi and
  • Paolo de Bernardis

Beilstein J. Nanotechnol. 2024, 15, 26–36, doi:10.3762/bjnano.15.3

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  • sensitivity. Scanning electron microscopy (SEM) images of the sample LSPE VB 210/240 SINS1 No. 43 deposited at NNSTU were obtained using an electron microscope at the Collective Use Center of the IPM RAS (Figure 4a,b). The dimensions of the junctions can be precisely measured using SEM and compared with the
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Published 04 Jan 2024

TEM sample preparation of lithographically patterned permalloy nanostructures on silicon nitride membranes

  • Joshua Williams,
  • Michael I. Faley,
  • Joseph Vimal Vas,
  • Peng-Han Lu and
  • Rafal E. Dunin-Borkowski

Beilstein J. Nanotechnol. 2024, 15, 1–12, doi:10.3762/bjnano.15.1

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  • using three different fabrication methods: lift-off, ion beam etching (IBE), and stencil lithography. They were further analyzed using different instruments, including scanning electron microscopy, LTEM, and electron holography. A bilayer of positive PMMA resist was utilized in the first fabrication
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Published 02 Jan 2024

A combined gas-phase dissociative ionization, dissociative electron attachment and deposition study on the potential FEBID precursor [Au(CH3)2Cl]2

  • Elif Bilgilisoy,
  • Ali Kamali,
  • Thomas Xaver Gentner,
  • Gerd Ballmann,
  • Sjoerd Harder,
  • Hans-Peter Steinrück,
  • Hubertus Marbach and
  • Oddur Ingólfsson

Beilstein J. Nanotechnol. 2023, 14, 1178–1199, doi:10.3762/bjnano.14.98

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  • (500 nm)/Si(111) In this experiment, 4 × 4 µm2 FEBID structures were written with [Au(CH3)2Cl]2 as the precursor using an acceleration voltage of 5 keV and a beam current of 1.5 nA. The fabricated structures were examined with scanning electron microscopy (SEM) and Auger electron spectroscopy (AES
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Published 06 Dec 2023

Hierarchically patterned polyurethane microgrooves featuring nanopillars or nanoholes for neurite elongation and alignment

  • Lester Uy Vinzons,
  • Guo-Chung Dong and
  • Shu-Ping Lin

Beilstein J. Nanotechnol. 2023, 14, 1157–1168, doi:10.3762/bjnano.14.96

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  • Supporting Information File 1, Figure S2). Scanning electron microscopy (SEM) images (Figure 1C–E) confirm the featureless surface of flat PU and the ordered arrays of nanopillars and nanoholes on the nanopatterned films. For the PU nanopillar substrate, some short pillars occassionally appeared (Figure 1D
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Published 29 Nov 2023

Curcumin-loaded albumin submicron particles with potential as a cancer therapy: an in vitro study

  • Nittiya Suwannasom,
  • Netsai Sriaksorn,
  • Chutamas Thepmalee,
  • Krissana Khoothiam,
  • Ausanai Prapan,
  • Hans Bäumler and
  • Chonthida Thephinlap

Beilstein J. Nanotechnol. 2023, 14, 1127–1140, doi:10.3762/bjnano.14.93

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  • Instruments Ltd., Malvern, UK) at 25 °C. The suspensions of the MPs were diluted to the appropriate concentration with PBS, pH 7.4 (conductivity 18 mS/cm). The size and zeta potential values were expressed as mean ± standard deviation of at least three repeated measurements. Scanning electron microscopy The
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Published 21 Nov 2023

Sulfur nanocomposites with insecticidal effect for the control of Bactericera cockerelli

  • Lany S. Araujo-Yépez,
  • Juan O. Tigrero-Salas,
  • Vicente A. Delgado-Rodríguez,
  • Vladimir A. Aguirre-Yela and
  • Josué N. Villota-Méndez

Beilstein J. Nanotechnol. 2023, 14, 1106–1115, doi:10.3762/bjnano.14.91

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  • rosemary essential oils with the three concentrations of 0.25%, 0.5%, and 0.75%. The samples were characterized by UV–visible spectroscopy, energy-dispersive X-ray spectroscopy, transmission electron microscopy, and scanning electron microscopy. The insecticidal efficacy of the nanocomposites was evaluated
  • eucalyptus and rosemary at different concentrations. Characterizations were carried out through UV–visible spectroscopy, energy-dispersive X-ray spectroscopy (EDS), transmission electron microscopy (TEM), and scanning electron microscopy (SEM); also the insecticidal efficacy of the NCMPs for the control of
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Published 17 Nov 2023

Dual-heterodyne Kelvin probe force microscopy

  • Benjamin Grévin,
  • Fatima Husainy,
  • Dmitry Aldakov and
  • Cyril Aumaître

Beilstein J. Nanotechnol. 2023, 14, 1068–1084, doi:10.3762/bjnano.14.88

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Published 07 Nov 2023

Spatial mapping of photovoltage and light-induced displacement of on-chip coupled piezo/photodiodes by Kelvin probe force microscopy under modulated illumination

  • Zeinab Eftekhari,
  • Nasim Rezaei,
  • Hidde Stokkel,
  • Jian-Yao Zheng,
  • Andrea Cerreta,
  • Ilka Hermes,
  • Minh Nguyen,
  • Guus Rijnders and
  • Rebecca Saive

Beilstein J. Nanotechnol. 2023, 14, 1059–1067, doi:10.3762/bjnano.14.87

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  • -sectional scanning electron microscopy images can be found in [32]. The top view of the piezo/photodiode device is given in Figure 1a, where the inset represents the cross section of the device stack. Owing to the integration of PZT with silicon processing and operation at low voltages, this device can be
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Published 06 Nov 2023
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